A new glyme adduct of the lead bis-hexafluoroacetylacetonate, [Pb(hfa) 2·diglyme]2, (diglyme = CH3O(CH 2CH2O)2CH3) has been synthesized and characterized. In particular, [Pb(hfa)2·diglyme]2 has been characterized by single crystal X-ray diffraction studies, which revealed the dimeric nature of the adduct. The thermal analysis has demonstrated high volatility and good thermal stability with a low residue despite the dimeric nature of the adduct. Films deposited on SrTiO3 (100) substrate are (001) oriented at deposition temperature as low as 450°C.
A novel precursor for mocvd of lead oxide films: [Pb(hfa) 2·diglyme]2 complex
Malandrino G.;Lo Nigro R.;
2005-01-01
Abstract
A new glyme adduct of the lead bis-hexafluoroacetylacetonate, [Pb(hfa) 2·diglyme]2, (diglyme = CH3O(CH 2CH2O)2CH3) has been synthesized and characterized. In particular, [Pb(hfa)2·diglyme]2 has been characterized by single crystal X-ray diffraction studies, which revealed the dimeric nature of the adduct. The thermal analysis has demonstrated high volatility and good thermal stability with a low residue despite the dimeric nature of the adduct. Films deposited on SrTiO3 (100) substrate are (001) oriented at deposition temperature as low as 450°C.File in questo prodotto:
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