The title compound, C41H40N2O6S2, has been synthesised in good yield and was found to form a 1 : 1 inclusion compound with CHCl3 and other organic solvents. The crystal and molecular structure of the CHCl3 solvate has been determined by single crystal X-ray analysis and refined to an R-value of 0.034 for 3229 reflections. The compound is monoclinic, space group P2(1)/c, with a = 15.316(1), b = 14,515(1), c = 18.720(3) angstrom, beta = 101.98(1)-degrees, and Z = 4. One molecule of chloroform is included in the crystal lattice.
|Titolo:||SYNTHESIS OF N,N'-DITOSYL-8,19-DIMETHOXY-2,5-DIAZA-[6.1]-NAPHTHYL-CYCLOPHANE - CRYSTAL AND MOLECULAR-STRUCTURE OF ITS 1/1 CHLOROFORM SOLVATE|
|Data di pubblicazione:||1993|
|Appare nelle tipologie:||1.1 Articolo in rivista|